Microwave Assisted Synthesis of Polycrystalline Flower-like ZincOxide Nanostructure Using Dicationic Ionic Liquid

نویسندگان

  • , A. R. Mahjoub Department of Chemistry, Tarbiat Modares University, Tehran, I.R. Iran
  • E. Kowsari Department of Chemistry, Tarbiat Modares University, Tehran, I.R. Iran
  • I. Yavari Department of Chemistry, Tarbiat Modares University, Tehran, I.R. Iran
  • M. Movahedi Department of Chemistry, Tarbiat Modares University, Tehran, I.R. Iran
چکیده مقاله:

In this paper, synthesis of the flower-like zinc oxide was performed using microwave assisted dicationic ionic liquid [mmp(im)2 ]Br2 . The polycrystalline flower-like zinc oxide nanostructure was obtained when a suitable mole ratio (ionic liquid /zinc acetate) and short duration microwave was used. X-ray diffraction (XRD), scanning electron microscopy (SEM), and photoluminescence (PL) spectra were employed to characterize of the as-synthesized zinc oxide. The SEM image illustrates that the surface of flower-like zinc oxide is polycrystalline with nanoparticles of about 48 nm. The samples fabricated in presence and absence of ionic liquid exhibited (UV, green-yellow) and (UV, blue, green) emission, respectively, while Commercial ZnO exhibited UV and green emission. 

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

microwave assisted synthesis of polycrystalline flower-like zincoxide nanostructure using dicationic ionic liquid

in this paper, synthesis of the flower-like zinc oxide was performed using microwave assisted dicationic ionic liquid [mmp(im)2 ]br2 . the polycrystalline flower-like zinc oxide nanostructure was obtained when a suitable mole ratio (ionic liquid /zinc acetate) and short duration microwave was used. x-ray diffraction (xrd), scanning electron microscopy (sem), and photoluminescence (pl) spectra w...

متن کامل

Ionic Liquid assisted Synthesis of Zeolite-TON

An ionic liquid assisted strategy for the synthesis of zeolitic material is reported. This strategy is a solid state synthetic method and the ionic liquid is employed as structure directing agent. A TON-type zeolite, which contains one-dimensional 10-member-ring, is successfully synthesized with the assistance of the ionic liquid, 1-ethyl-3-methylimidazolium bromide. This finding improves our u...

متن کامل

Controllable Synthesis of Flower-Like ZnO Nanostructure with Hydrothermal Method (RESEARCH NOTE)

Flower-like ZnO nanostructures were synthesized by decomposing Zn(OH)2 in 1,4- butanediol at 105 °C for 36 h. Size of flower-like ZnO nanostructure can be controlled by pH of the aqueous solution. In the preparation of flower-like ZnO nanostructure, zinc nitrate was used as a precursor. The morphology and microstructure of flower-like ZnO nanostructure have been characterized by scanning electr...

متن کامل

Dicationic Ionic Liquid as the Recyclable Catalyst for the Synthesis of Quinoxaline Derivatives

An efficient and eco-friendly protocol for the synthesis of quinoxaline derivatives employing a condensation reaction between 1,2-diketone and 1,2-diaminobenzene derivative has been developed. The reaction of  1,2-diketone and 1,2-diaminobenzene derivative was carried out in water at room temperature using 10 mol% of task-specific dicationic ionic liquid as a catalyst. The results show that...

متن کامل

Synthesis of Novel Flower-Like Zn(OH)F via a Microwave-Assisted Ionic Liquid Route and Transformation into Nanoporous ZnO by Heat Treatment

Zinc hydroxide fluoride (Zn(OH)F) with novel flower-like morphology has been prepared via a microwave-assisted ionic liquid route. The flower-like Zn(OH)F particle has six petals and every petal is composed of lots of acicular nano-structure. Nanoporous ZnO is obtained by thermal decomposition of as-prepared Zn(OH)F in air, and the flower-like morphology is well retained. In the process of synt...

متن کامل

One-pot synthesis of 2,4,5-trisubstituted imidazoles catalyzed by dicationic magnetic room temperature ionic liquid

Regarding the green chemistry's goals, dicationic magnetic room temperature ionic liquid open up new avenue to introduce an amazing and efficient system for facilitating catalyst recovery in different organic reactions. Ability of this dicationic magnetic room temperature ionic liquid catalyst in the one-pot three-components condensation reaction of benzil, aromatic aldehyde, and ammonium aceta...

متن کامل

منابع من

با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ذخیره در منابع من قبلا به منابع من ذحیره شده

{@ msg_add @}


عنوان ژورنال

دوره 6  شماره 4

صفحات  216- 222

تاریخ انتشار 2010-12-01

با دنبال کردن یک ژورنال هنگامی که شماره جدید این ژورنال منتشر می شود به شما از طریق ایمیل اطلاع داده می شود.

میزبانی شده توسط پلتفرم ابری doprax.com

copyright © 2015-2023